Journal of Liaoning Petrochemical University
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Treatment of Oily Sludge in Oil Field With Hot Water Washing
ZHAO Yang, DAI Yue-ling, LI Xiao-ou, LI Dong-sheng, QIN Yong-hang
Abstract565)      PDF (254KB)(490)      
 
The Oil Sludge of Liaohe oil field was cleaned and treated by hot water. The optimum reagent was selected by comparison, and the effect of experimental conditions (including the concentration of reagent, mass ratio of liquid to soil, stirring rate, slurry time and temperature) on oil yield were studied; and the best experimental conditions are obtained as follows: reagent concentration 4%, slurry time 25 min, slurry temperature 60 ℃, mass ratio of liquid to soil 4∶1 and stirring rate 200 r/min. Under these conditions, Oil yield can reach 94.29% after treating oil sludge once. The slurry solution can be recycled; the crude oil separated can be recycled after treatment.
2011, 31 (2): 14-16. DOI: 10.3696/j.issn.1672-6952.2011.02.005
Removal of Basic Nitrogen of Coker Gatch
ZHAO Qi-long,LI Dong-sheng*, LI Xiao-ou
Abstract404)      PDF (411KB)(325)      
 
Using a kind of compound solvent as denitrification agent to remove the basic nitrogen of CGO .Different process conditions including reaction temperature, denitrification agent to CGO mass ratio and reaction time on the effect of basic nitrogen remove rate and the light oil yield were studied.The experimental results show that the oil yield was 94.23% , and the basic nitrogen remove rate reached to 85.62% under the conditions of the reaction temperature 72 ℃ , the solvent to oil mass ratio 2.5%, the stirring speed 300 r/min , the reaction time 30 min and the settling time 15 min,which is the best reaction condition.
2010, 30 (1): 19-22. DOI: 10.3696/j.issn.1672-6952.2010.01.006
Exploitation and Research of the Water Soluble Imidazolinylquaternary-Ammonium-Salt Corrosion Inhibitor
SUN Ling-ling, LI Dong-sheng, LI Xiao-ou, LIU Jie, WANG Hui
Abstract489)      PDF (198KB)(392)      
Exploitation and research of compositive product, i.e. Corrosion Inhibitor, was carried out by the mixing of the main component of corrosion inhibitor with surfactants, chelate, organic amine and liquid of prefabrication, then the optimal proportion was found out in order to build the best matching systems. The models among the anti-corrosive capacity of the inhibitor and operation conditions were established by polynary quadratic regression. The optimum operation conditions obtained by non-linear programming (NLP) are the following: the amount of the surfactants, chelate, organic amine and the liquid of prefabrication is 0.112 6, 0.010 2, 0.213 9 and 0.357 2 respectively. The verified experiment showed that the products under the optimum operation conditions had the better water-soluble capablity, slower corrosion rate and higher anti-corrosive capacity (up to over 99%).
2008, 28 (4): 16-19.
Non-Hydrogen-Dewaxing Catalyst for Hydrocracked Tail Oil
ZHANG Ai-min, LIU jie, SONG Yi, LI Dong-sheng, ZHAI Yu-chun
Abstract373)      PDF (141KB)(212)      
The catalytic performance of self- developed non-hydrogen-dewaxing catalyst (FC-DB) was evaluated, and the hydrocracking tail oil was used as feed stock. The influence of reaction temperature and space velocity on the yield and pouring point of base oil was investigated. The relationships between yield, pouring point and operation conditions were determined by polynary quadratic regression, and the optimum operation conditions were determined by non-linear programming. The reaction temperature is 400 ℃ and space velocity is 1.2 h-1. At this time, the yield and pouring point of base oil respectively are 92.53% and -20 ℃, approximately dropping 53 ℃. The qualify of base oil obtained under above optimum operation conditions was analyzed, and the base oil can be used as premium lubricant base oil because of its high viscosity index, low pouring point, acidity and residue carbon.
2007, 27 (3): 21-24.